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41 Similarly Gotfredsen et al reported that only 16 nmol loading of an octapeptide onto a resin was required to obtain a high-resolution 1H spectrum of the peptide (still bound to the resin) within 20 minutes42 Quantitation was achieved by uorescence Three times greater loading was required for complete structural elucidation by NMR42 After cleaving the peptide and analyzing by NMR in a small-volume probe, the 1H solution-state spectrum revealed the presence of isomers whose resonances were unresolved in the spectra acquired on the bead42 The isomers may have been detected in the 13C spectrum, where greater chemical shift dispersion improves resolution Such an observation was made by Anderson et al, who used GC analysis of cleaved product to con rm the exo/endo isomeric ratio of norbornane-2-carboxylic acid inferred by relative peak intensities in the on-bead 13C NMR spectrum.

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By administering tests via computer, test developers are provided with more leeway in the types of question they can ask than with traditional paper-andpencil tests, which are well suited to multiple-choice questions In a comprehensive review of the literature on computerized testing, Zenisky and Sireci (2002) identi ed over 20 new types of item format Some examples f novel item formats for computer testing include graphical modeling, mathematical expressions, generating examples, multiple numerical responses, passage editing, and problem-solving vignettes In this section, a brief description along with an example will be provided for each of these novel item formats Graphical modeling, mathematical expressions, and generating examples can all be classi ed as novel ways to assess mathematical ability (Bennett, Morley, & Quardt, 2000) Historically, math tests included in large-scale testing programs such as the Scholastic Aptitude Test (SAT) and the American College Testing (ACT) program were composed of selected response items; however, graphical modeling, mathematical expressions, and generating examples represent three alternative assessment formats for mathematical ability that use a constructed response approach With graphical modeling (GM) items, examinees are given a brief description of a mathematical problem and asked to plot this information on a grid so that it represents the information provided For example, an examinee may be asked to plot points on a grid for a circle with an area equal to 16 As in this problem, it is possible to have more than one correct answer; consequently scoring becomes a challenge for the test developer While completing mathematical expression (ME) items, examinees are asked to construct a mathematical equation that represents the problem (Bennett et al, 2000) For example, if n is the arithmetic mean of three numbers 3, 5, and j, what is the value of j in terms of n (Solution: j 3n 3 5) Again, a critical issue for mathematical expression items is scoring: there can be any number of ways to write equally correct equations An important contribution of Bennett et al (2000) is their scoring algorithm They used symbolic computation principles to convert alternative answers to a simplest form, which could then be compared with the answer key In a test of the scoring algorithm, they found it correctly scored answers with an accuracy of greater than 996%; moreover, most of the answers that were classi ed as incorrectly scored by the algorithm contained problematic subscripts (eg X1 rather than X1) Like ME items, generating examples (GE) items set constraints within the problem and then ask the examinee to give an equation or value that meets these constraints (Bennett et al, 2000) For example, if a and b are positive integers and 5a 3b 1, what are two possible sets of value for a and b (Solution: a 2; b 3; a 5; b 8) By assessing mathematical ability with constructed response items, the construct of mathematical ability is broadened to incorporate and assess skills not feasible with a traditional multiple-choice format.

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43 The tether carbons of the polystyrene resin were also observed in this example, which provided an internal standard for determining the extent of reaction completion43 Riedl et al were able to determine the enantiomeric excess of diasteroemeric Mosher esters by 13C HR-MAS NMR44 The results obtained using seven pairs of 13C resonances agreed within <1% with results obtained by HPLC on the cleaved products44 Lacey et al used a solenoidal microcoil probe with an active volume of 800 nL to measure 1 H NMR spectra of a compound cleaved from a single solid-phase resin bead in one hour45 The amount of product cleaved from the bead was determined using an internal standard to be around 500 pmol, in good agreement with the loading capacities provided by the manufacturer of the Tentagel resin Related: .

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RPRs are a metro-oriented technology intended to be more data-friendly and cost-effective than SONET/SDH They are primarily being developed by the IEEE 80217 Working Group, although there is a coordinating IP over RPR working group in the IETF s sub-IP area and an industry forum, the RPR Alliance, is being formed One of the major goals of RPRs is to have the fast protection switching of SONET, but using the capacity of the alternate ring for traffic rather than merely for backup Of course, if one ring fails, either some low-priority traffic will be dropped or the ring s performance will degrade The actual RPR technology is a layer 2 Medium Access Control protocol, which can operate over the same physical facilities as SONET, but also 10Gigabit Ethernet and new physical media ith respect to SONET, it replaces the framing and the protection mechanisms As opposed to Ethernet, it offers protection switching at SONET speeds Metropolitan area networks (MANs), and RPRs in general, are intended to smooth some of the disconnects between enterprise-oriented LANs and long-haul SONET/DWDM [Vijeh 2000] RPR technology is agnostic of the specific underlying transmission technology The. Code 128A Printer In VS .NET Using Barcode maker for .Related: EAN-8 Generation VB.NET , .NET Intelligent Mail Generating , Create UPC-A .NET

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in .NET Printer QR Code in .NET This code creates the ML declaration and inserts it before all other child nodes. using barcode printing for web control to generate, create qr .Format( {0} <b>Type:</b>{1} <b>Name:</ b>{2} <b>Attr:</b> , _ New String( - , level node.NodeType, node.Name) If node.HasAttributes Then node.MoveToFirstAttribute() Do s &= s.Format( {0}={1} , node.Name, node.Value) Loop While node.MoveToNextAttribute() node.MoveToParent() End If Response.Write(s & <br> ) If node.HasChildren Then node.MoveToFirstChild() Do RecurseNavNodes(node, level + 1) Loop While node.MoveToNext() node.MoveToParent() End If End Sub.Related: ISBN Generating Word , Create UPC-A Java , Interleaved 2 of 5 Generator VB.NET

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