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Compared with the corresponding bulk materials, the structural characterization of thin, self-assembled lms prepared by EISA imposes certain complications The analysis of structural parameters such as the pore size distribution, the pore volume, and the type of mesostructure (eg, lamellae and cubic) is complicated mainly by the low amount of material but also by factors resulting from the lm geometry itself For instance, self-assembled lms often show a preferred orientation of the mesostructure with respect to the substrate, which can only be discerned by appropriate techniques adapted to lms, especially grazing incidence X-ray analysis In particular, major insights into the selfaggregation process can be achieved by in situ methods following the structure formation in real time.

similar to that observed for CuInS2 deposited at 450 C.40 The variation in lm composition is understandable since the two precursor thermal decomposition pro les are dissimilar. Therefore, using two SSPs with matching thermal pro les might provide a more effective means for depositing quaternary lms. 6.3.3 Impact of Reactor Design on CuInS2 Film Growth

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Among other methods, 2D-GISAXS (grazing incidence small-angle X-ray scattering), SRSAXS (SAXS in symmetric re ection), X-ray re ectometry, wide-angle X-ray scattering (WAXS), ellipsoporosimetric porosimetry, (high-resolution) transmission electron microscopy, time-resolved infrared spectroscopy, surface acoustic waves (SAW), and optically polarized xenon nuclear magnetic resonance (NMR) have proven to be highly relevant for this purpose Since the advances in the preparation of self-assembled thin lms is strongly based on the parallel progress in appropriate characterization techniques, in the following sections, several of these novel analytical methods are described, which were speci cally designed for thin- lm analysis 931 Positron Annihilation Lifetime Spectroscopy (PALS) PALS is sensitive to different kinds of defects, such as dislocations, grain boundaries, voids, and pores Similar to most scattering techniques, PALS is a noninvasive technique, thereby allowing for the detection of inaccessible pores, and it is suf ciently sensitive to determine the porosity in thin lms.

Summary

PALS is based on the decay of positrons into two photons ( annihilation )22 Entering the sample, the positrons (eg, created by a 22Na radioactive source) lose their energy by inelastic collisions with electrons These thermalized positrons have energies on the order of a few meV and form positroniums (Ps, the electron positron bound state), which diffuse through the solid until annihilation after their lifetime The natural lifetime of Ps (ie, 142 ns) is reduced by annihilation with electrons during collisions and, thus, becomes longer when a positron or positronium is localized at spaces with lower electron density, such as voids Therefore, positrons can be used as a probe to investigate the average sizes of the free volume, size distribution, and the free volume concentration by measuring their lifetimes23 Since the determination of pore.

The Wrap feature enables you to wrap 2D sketches around cylindrical and conical faces. However, trying to wrap around 360 degrees can cause some difficulties. Although all of the available information on the Wrap feature says that you can wrap onto a conical surface, it fails to mention that the point of the cone must be cut off in order for it to work. The Wrap feature works by flattening the face, relating the sketch to the flat pattern of the face, and then mapping the face boundaries and sketch back onto the 3D face. The reason why it is limited to cylindrical and conical faces is that these types of geometry are developable. This means that the faces can be mapped to the flat pattern through some relatively simple techniques that happen behind the scenes. Developable geometry can be flattened without stretching. You will see in a later chapter that sheet metal functions are limited in the same way and for the same reasons. SolidWorks does not wrap onto other types of surfaces, such as spherical, toroidal, or general NURBS surfaces, because you cannot flatten these shapes without distorting or stretching the material. There is software that can flatten these shapes, but it is typically done for sheet-metal deep drawing applications, which highly deform the metal. The Wrap feature has three main options: n Emboss n Deboss n Scribe Figure 7.52 shows the Wrap PropertyManager interface.

The Edit Block toolbar button on the Blocks toolbar The Edit button in the Block PropertyManager Choosing Tools Block Edit from the menus From the RMB menu of the block in the Blocks folder in the drawing FeatureManager

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